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A novel and efficient Fe‐catalyzed direct C−H amination (NH2) of arenes is reported using a new redox‐active aminating reagent. The reaction is simple, and can be performed under air, mild, and redox‐neutral conditions. This protocol has a broad substrate scope and could be used in the late‐stage modification of bioactive compounds. Mechanistic studies demonstrate that a radical pathway could be involved...
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