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A 3D porous perchlorinated metal–organic framework (MOF), LIFM‐26, featuring dual functionality, that is, functional polar groups and open metal sites, has been synthesized using perchlorinated linear dicarboxylate to link trigonal prismatic Fe3(μ3‐O) units. LIFM‐26 exhibits good thermal and chemical stability, and possesses high porosity with a BET surface area of 1513 m2 g−1, compared with isoreticular...
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