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We report the synthesis and characterization of new NixRu1−x (x=0.56–0.74) alloy nanoparticles (NPs) and their catalytic activity for hydrogen release in the ammonia borane hydrolysis process. The alloy NPs were obtained by wet‐chemistry method using a rapid lithium triethylborohydride reduction of Ni2+ and Ru3+ precursors in oleylamine. The nature of each alloy sample was fully characterized by TEM,...
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