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A new approach for gas‐phase modification of ultra‐high‐molecular‐weight polyethylene (UHMWPE) film for synthesis of proton exchange membranes (PEMs) has been successfully realized. First, the membrane precursors have been prepared by soaking the films in a monomers/AIBN solution followed by their modification with polystyrene (PS) in styrene vapor at 110°C. The developed method is characterized by...