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Developing graphene‐like two‐dimensional materials naturally possessing a band gap has sparked enormous interest. Thanks to the inherent wide band gap and high mobility in the 2D plane, covalent organic frameworks containing triazine rings (t‐COFs) hold great promise in this regard, whilst the synthesis of single‐layer t‐COFs remains highly challenging. Herein, we present the fabrication of a well‐defined...
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