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Low temperature and atmospheric pressure plasma‐induced polymerization was demonstrated as a fast and facile strategy for tailoring of packing phase of COF‐1 as well as preparing diverse covalent organic frameworks (COFs) including both two‐dimensional (2D) COFs and three‐dimensional (3D) COFs. By regulating the solvents, the fast construction of well‐ordered AB staggered COF‐1 and AA eclipsed COF‐1...
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