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A rapid and scalable synthesis of six new imine‐linked highly porous and crystalline COFs is presented that feature exceptionally high chemical stability in harsh environments including conc. H2SO4 (18 m), conc. HCl (12 m), and NaOH (9 m). This is because of the presence of strong interlayer C−H⋅⋅⋅N hydrogen bonding among the individual layers, which provides significant steric hindrance and a hydrophobic...
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