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A functional model complex of nickel superoxide dismutase (NiSOD) with a non‐peptide ligand which mimics the full catalytic cycle of NiSOD is unknown. Similarly, it has not been fully elucidated whether NiSOD activity is a result of an outer‐ or inner‐sphere electron‐transfer mechanism. With this in mind, two octahedral nickel(II)/(III) complexes of a bis‐tridentate N2S donor carboxamide ligand, N...
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