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The selective decarbonylation of formic acid was achieved under transition‐metal‐free conditions. Using a liquid chemical‐looping strategy, the thermodynamically favored dehydrogenation of formic acid was shut down, yielding a pure stream of CO with no H2 or CO2 contamination. The transformation involves a two‐step sequence where methanol is used as a recyclable looping agent to yield methylformate,...
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