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Die Makrocyclisierung ist üblicherweise der Schlüsselschritt in der Synthese von Naturstoffen des Typs Cyclophan. Betrachtet man Cyclophane mit axial chiralen Biaryleinheiten, so ist die Kontrolle der Atropselektivität – hinsichtlich Synthese und biologischen Aktivitäten – wesentlich und herausfordernd. Wir berichten über einen atropselektiven Zugang via Heck‐Cyclisierung, der erstmals die Totalsynthese...
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