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An olefin‐assisted palladium‐catalyzed oxidative carbocyclization–alkoxycarbonylation of bisallenes to afford seven‐membered carbocycles has been established. This dehydrogenative coupling reaction showed excellent substrate scope and functional group compatibility. The reaction exhibited high chemo‐ and regioselectivity, and ester 3 was the only product obtained. The olefin unit has been proven to...
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