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A precious‐metal‐ and Cd‐free photocatalyst system for efficient H2 evolution from aqueous protons with a performance comparable to Cd‐based quantum dots is presented. Rod‐shaped ZnSe nanocrystals (nanorods, NRs) with a Ni(BF4)2 co‐catalyst suspended in aqueous ascorbic acid evolve H2 with an activity up to 54±2 mmol
gZnSe−1 h−1 and a quantum yield of 50±4 % (λ=400 nm) under visible light illumination...
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