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The selective construction of P−C bonds directly from P4 and nucleophiles is an ideal and step‐economical approach to utilizing elemental P4 for the straightforward synthesis of organophosphorus compounds. In this work, a highly efficient one‐pot reaction between P4 and 1,4‐dilithio‐1,3‐butadienes was realized, which quantitatively affords phospholyl lithium derivatives. DFT calculations indicate...
Coupling of carbon monoxide with nitrogen monoxide was achieved at a frustrated Lewis pair template. This unique reaction uses hydride as an auxiliary, which reductively activates carbon monoxide at the frustrated Lewis pair. The CO/NO coupling reaction then takes place through a pathway involving a radical reaction in which the hydrogen atom auxiliary is eventually removed again.
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