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Tetrakis(dimethoxyphenyl)adamantane (TDA) readily forms crystalline inclusion complexes with reactive, toxic, or malodorous reagents, such as benzoyl chloride, acetyl chloride, cyclohexyl isocyanide, phosphorus trichloride, and trimethylsilyl chloride. The crystals are stable and largely free of the problematic properties of the free reagents. When exposed to solvents such as DMSO or MeOH, the reagents...
Die Verkapselung aggressiver Reagentien in organischen Kristallen vereinfacht deren Handhabung, während ihre Reaktivität bei Freisetzung in einem passenden Lösungsmittel wiederhergestellt wird. In der Zuschrift auf S. 13910 ff. zeigen C. Richert et al., dass z. B. Benzoylchlorid, PCl3 und Cyclohexylisocyanid in Kristallen von Tetrakis(dimethoxyphenyl)adamantan eingeschlossen werden können. Das Titelbild...
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