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A method to introduce high‐index facets into colloidally synthesized nanoparticles is used to produce compositionally uniform Pt–M (M = Ni, Co, and Cu) and Rh–M (M = Ni and Co) tetrahexahedral nanoparticles. The realization of this method allows for a systematic study of catalyst activity as a function of particle composition for various electrooxidation reactions of liquid fuels (formic acid, methanol,...
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