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The oxidation of intracellular biomolecules by reactive oxygen species (ROS) forms the basis for ROS‐based tumor therapy. However, the current therapeutic modalities cannot catalyze H2O2 and O2 concurrently for ROS generation, thereby leading to unsatisfactory therapeutic efficacy. Herein, it is reported a bioinspired hollow N‐doped carbon sphere doped with a single‐atom copper species (Cu‐HNCS) that...
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