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In the reaction of cis- and trans-2-n-alky-5-hydroxyl-1,3-dioxane mixtures with SO3 · pyridine complex, followed by neutralization with sodium hydroxide or sodium carbonate, a new group of anionic surfactants, i.e., sodium cis- and trans-(2-n-alkyl-1,3-dioxan-5-yl)sulfates were obtained. The hydrophobic intermediates used in the sulfation reaction were obtained in high yields from four-component glycerol...
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