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Spherical LiNi1/3Co1/3Mn1/3O2 was successfully prepared by controlled crystallization. The preparation started with the spherical coprecipitate of Ni1/3Co1/3Mn1/3CO3 from NiSO4, CoSO4, MnSO4, NH4HCO3, and NH3·H2O, followed by pyrolysis of Ni1/3Co1/3Mn1/3CO3 at 600°C for 3 h. The X-ray diffraction analysis showed that the homogeneous cubic (Ni1/3Co1/3Mn1/3)3O4 was obtained after the pyrolysis. Spherical...
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