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Isothermal conditions are a prerequisite for the accurate determination of kinetics in heterogeneous catalysis. In this work, an integral fixed-bed lab reactor with 5 mm inner diameter placed inside an aluminum heating block is used. Temperature profiles were recorded with a single but axially movable thermocouple in a fixed bed of a highly loaded supported Ni catalyst (15.4 wt% Ni on γ-Al2O3) for...
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