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In this study, a set of multilayer hard nanocrystalline coatings of Al/AlN with 35, 55 and 75 bilayer were prepared by DC magnetron sputtering on AISI 52100 steel specimens at nitrogen fractions of 35 and 65% in the Ar + N2 discharge. X-ray diffraction analysis indicates a polycrystalline structure of AlN + Al and AlN phases for 35% N2 and 65% N2 fraction, respectively. Nanoindentation tests showed...
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