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The analyses of 99gTc-DMSA complexes prepared under alkali and acidic reactions were reported. Modern analytical, separation and spectral methods such as NMR (1H-NMR, 13C-NMR, APT, COSY and HSQC) and Q-TOF HPLC–MS/MS system with ESI were employed to determine the identity and characterization of the products. The structure of 99gTc(V)DMSA was clearly confirmed and its fragmentation path in negative...
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