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The thermal decomposition of M3[Fe(cit)2]2 4H2O (M = Sr, Ba) has been studied isothermally and non-isothermally employing simultaneous (TG–DTG–DSC), XRD, IR, SEM and Mössbauer spectroscopic techniques. The anhydrous complexes decompose at 140–220°C to yield α-Fe2O3 and MC5H4O5 (metal acetone-dicarboxylate) intermediates. The latter decomposes to respective carbonate at higher temperature. α-Fe2O3...
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