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Fe–ZSM-5 catalysts are prepared by FeCl3 sublimation between 320 and 850 °C. The catalysts are characterised by XRD, H2–TPR, NH3–TPD, NO adsorption by DRIFTs, and catalytic activity is evaluated for N2O decomposition. The influence of high temperature (850 °C) and pretreatment environment (air, He, He+H2O and H2) on the nature of iron species in Fe–ZSM-5 is further investigated by DRIFTs. High temperature...
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