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Comparative gas chromatographic applications of two new liquid crystals were investigated. The characterization of the two mesogenic compounds was performed with 1H NMR and mass spectrometry. The thermal properties were established by differential scanning calorimetry. The optical characterization of the liquid crystal was made by using polarizing optical microscopy. The chromatographic separation...
The dicarbonyl compounds glyoxal, methylglyoxal, and dimethylglyoxal have been separated by capillary GC on a 30 m × 0.32 mm i.d. HP-5 column after precolumn derivatization with 2,3-diamino-2,3-dimethylbutane at pH 4. Chromatographic separation was complete in 6 min. Nitrogen was used as carrier gas at a flow rate of 2 mL min−1. Split injection was performed with a split ratio of 10:1 (v/v). The derivatives...
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