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A novel, sensitive and simple liquid chromatography method with charged aerosol detection (LC-CAD) for the simultaneous assay determination of pancuronium and its impurities (dacuronium and vecuronium) has been developed. The limit of quantitation for vecuronium and dacuronium was 1.64 and 3.42 μg mL−1, respectively. The elaborated method was validated for linearity, precision and accuracy. This LC-CAD...
A new, simple and repeatable liquid chromatography method with charged aerosol detection (LC-CAD) for the determination of gentamicin sulphate composition and related substances has been developed. Gentamicin lacks of chromophores, therefore its determination is quite problematic. Using a universal CAD enables to achieve good separation without sample derivatization. Mass spectrometry was employed...
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