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Electrochemical oxidation of thiocyanate (SCN−) on platinum electrode in the sulfuric acid medium was studied using cyclic voltammetry, in situ UV-visible absorption measurement, rotating ring-disc electrode voltammetry, and electrical impedance spectroscopy. Two oxidation processes are involved in the electrochemical oxidation of SCN− in sulfuric acid medium. The adsorbed SCN− undergoes oxidation...
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