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The hydrolysis of SbCl3 in hydrochloric acid solution (2.0 mol dm−3 HCl) at 0 °C yields an amorphous product consisting of uniform spherical particles (d∼0.5 µm), which on continuous aging at the same temperature transform to larger crystals, indicated by XRD to be Sb4O5Cl2. In contrast, in the same solution kept at 25 °C crystalline particles of the same composition form directly after an induction...
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