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Hydroxyl radicals (OH), together with carbon-centered radicals (R), derived from photoinduced electron transfer (PET) interactions between viologen and carboxylic acid ion pairs ([bipy++⋯RCOOH]), were developed to photoinitiate the polymerization of various acrylate monomers in the presence of oxygen. The mechanism of the radicals’ formation was established using nanosecond laser flash photolysis...
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