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The recovery and separation of cobalt and manganese were investigated according to ion exchanger properties and pH of solutions. It was determined that cobalt sorption increases with pH increase to 5.5. The cobalt and manganese separation is performed using manganese substitution by cobalt ions at pH more than 3.5 on chelating resins ANKB-35 and AMF-2M. The cobalt content of manganese sulphate solutions does not exceed 0.6 mg/1.