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The oxidation of hydroxyurea (H2NCONHOH, HU) at Au(100), Au(111) and Au(111)–25nm thin film electrodes is studied spectroelectrochemically in perchloric acid solutions. HU, which in agreement with DFT results interacts weakly with the gold surfaces, oxidizes irreversibly at gold electrodes irrespective of the surface orientation. The in situ infrared external reflection spectra prove the formation...
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