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An efficient stereoselective synthesis of Z-stilbenes has been developed from diarylalkynes via a new hydrosilylation–protodesilylation process. The scope and limitation of this method is presented to stereoselectively prepare a wide range of (Z)-stilbenes in a one-pot way is presented. A concise application to the preparation of combretastatin A-4 (CA-4), a vascular targeting agent inhibitor of tubulin...
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