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An in-depth analysis of the development of small angle X-ray scattering (SAXS) data of ordered mesoporous materials (OMM) upon continuous modification of the material is presented. Two cases are considered here: in situ SAXS pattern of the decomposition of MCM-41 with a 1M solution of NaOH and the calcination of Pd/TiO 2 nanocomposite material at different temperatures. In both cases the modification...
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