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Catalytic reduction of CO2 (saturated in organic polar solvents, e.g. N,N-dimethylfomamide, containing Me4NX or NaBF4) was achieved at smooth gold electrodes and at glassy carbon electrodes galvanostatically capped with a thin layer of gold. Under these quite explicit conditions, very sharp reduction steps were observed near −1.5V vs. Ag/AgCl. With small cations listed above, an unexpected behavior...
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