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Glassy carbon was reported to be efficient in two-electron reductive scission of alkyl halides RX for leading to RH. When organic solvents are used, it is shown that, within the potential range [−1.5V to −3V], the electrochemical process is complicated to a large extend by the progressive alkylation of the carbon surface until the formation of compact films composed of immobilized alkyl groups. It...
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