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Highly crystallized BaMoO 4 films have been prepared on a molybdenum substrate in an alkaline solution containing barium ions at room temperature (25°C). The film formation is based on a solution reaction assisted by an electrochemical dissolution of metal molybdenum. The film (thickness 3 μm) was polycrystalline with a grain size of about 6 μm. The film morphology is related to the nucleation and growth behavior of the BaMoO 4 particles on a molybdenum metal substrate.