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A hydrothermal route has been adopted to prepare metastable wurtzite-type (γ) manganese sulfide (MnS) crystallites via the reaction of manganese acetate (Mn(CH 3 COO) 2 ) and thioacetamide in water at 60-130 o C. Experiments show that the control of reaction temperature and time is important to the target phase. It is suggested that kinetics plays a predominant role in the formation of γ-MnS under the hydrothermal conditions.