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The nanostructure of a nanocrystalline Fe 73.5 Si 13.5 B 9 Nb 3 Cu alloy has been studied by means of Mössbauer spectroscopy, 1D and 3D atom probes. After 6h at 520°C, the crystallized fraction of the alloy is about 53%. α-Fe(Si) nanocrystals, 10–20nm in diameter, are embedded in a retained amorphous matrix. They have a near Fe 80 Si 20 composition and...
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