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We used X-ray diffraction, small-angle X-ray scattering, and scanning electron microscopy (SEM) to study the diamond graphite phase transition in detonation nanodiamond (ND) intercalated with Cu, Ni, Co and Fe for the first time. The study has been made before and after annealing in hydrogen and argon. The SEM data obtained support the idea of the hierarchic structure of ND with a size of primary...
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