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The toxicity and bioaccumulation of organotin compounds (OTCs) led to the development of sensitive and selective analytical methods for their determination. In the past much attention was assigned to the study of OTCs in biological samples, water and sediments, coming mostly from marine environment. Little information about OTCs pollution of terrestrial ecosystems is available. In order to optimise...
A new ultra high-performance liquid chromatography method with UV detection was examined for detection and separation of polychlorinated biphenyls. This included optimization of separation conditions for two model mixtures containing seven and fifteen most relevant congeners, comparison of three types of reversed phase sub-2-micron particle sized columns and assessment of system suitability under...
A fingerprinting approach was developed by means of gas chromatography–mass spectrometry (GC–MS) and IR spectroscopy for quality control of Portulaca oleracea L., a traditional Chinese food and medicine that has been used for thousands of years in China. Eleven P. oleracea L. samples obtained from different sources were used to establish the fingerprints, and the similarity evaluation and hierarchical...
A method was developed for the simultaneous analysis of 14 pesticide residues (clofentezine, carbofuran, diazinon, methyl parathion, malathion, fenthion, thiabendazole, imazalil, bifenthrin, permethrin, prochloraz, pyraclostrobin, difenoconazole and azoxystrobin) in mango fruit, based on solid-phase micro extraction (SPME) coupled to gas chromatography–mass spectrometry (GC–MS). Different parameters...
A rapid, economic and environmentally friendly analytical methodology has been implemented for the determination of α-, β-, γ- and δ-HCH, p,p′-DDT, p,p′-DDD and p,p′-DDE, PCBs congeners #28, #52, #101, #153, #138 and #180 and Hexachlorobenzene in fish oil. 1,2,3,4-Tetrachloronaphtalene was used as internal standard. The sample preparation, consisting of a single step of clean-up and fractionation,...
A procedure based on capillary column gas chromatographic–mass spectrometric (GC–MS) confirmation was developed for the verification of the ubiquitous and versatile chemical and nerve agent simulant, dimethyl methyl phosphonate (DMMP; CAS# 756-79-6), from gaseous samples. This method was developed to verify low nanogram DMMP concentrations during testing of a nerve agent detection system. Standard...
Landfill or digester gas can contain man-made volatile methylsiloxanes (VMS), usually in the range of a few milligrams per normal cubic metre (Nm 3 ). Until now, no standard method for siloxane quantification exists and there is controversy with respect to which sampling procedure is most suitable. This paper presents an analytical and a sampling procedure for the quantification of common...
The analysis of hydrocarbons in chert rocks provides a worthwhile source of information regarding the geochemical features of a depositional setting. Since the typical analytical procedure requires long Soxhlet extractions and the use of large quantities of sample (30–50g), in this work we have optimised the focused ultrasound extraction (FUSE) and the microwave-assisted extraction (MAE) to make available...
In this work, a straightforward, reliable and effective automated method has been developed for the direct determination of monoaromatic volatile BTEXS group (namely benzene, toluene, ethylbenzene, o-, m- and p-xylenes, and styrene) in olives and olive oil, based on headspace technique. Separation, identification and quantitation were carried out by headspace-gas chromatography–mass spectrometry (HS-GC–MS)...
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