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An excellent electrochemical sensing platform has been designed by combining the huge specific surface area of carbon nanotubes (CNTs) and the remarkable conductivity of ionic liquid (IL). IL can easily untangle CNTs bundles and disperse CNTs by itself under grinding condition due to the π–π interaction between CNTs and IL. The resulting nanocomposites showed an augmentation on the voltammetric and...
The paper presents application of multiwall carbon nanotubes (MWCNTs) modified with 5-dodecylsalicylaldoxime to copper(II) flow-injection on-line preconcentration and flame atomic absorption spectrometric (FAAS) determination. Two new sorbents were obtained by impregnation of MWCNTs with Cu(II)-LIX 622 ® complex, however in the first case modification was preceded by carbon wall activation...
Amperometric flow injection method of hydrogen peroxide analysis was developed based on catalase enzyme (CAT) immobilization on a glassy carbon electrode (GC) modified with electrochemically deposited gold nanoparticles on a multiwalled carbon nanotubes/chitosan film.The resulting biosensor was applied to detect hydrogen peroxide with a linear response range 1.0×10 −7 –2.5×10 −3 M...
A novel carbon paste electrode based on functionlized multi-walled carbon nanotubes/β-cyclodextrin composite (FMWCNTs/β-CD-CPE) is described for potentiometric determination of piroxicam (PXM). Improved sensitivity and selectivity was achieved by application of CDs as molecular host–guest recognition elements and MWCNTs. The electrochemical performance of carbon paste electrodes incroporated with...
A biosensor based on atemoya peroxidase immobilised on modified nanoclay was developed for the determination of glyphosate by the enzyme inhibition method. The inhibitor effect of the biocide results in a decrease in the current response of the hydroquinone that was used as a phenolic substrate to obtain the base signal. The biosensor was constructed using graphite powder, multiwalled carbon nanotubes,...
In this work, the multi-walled carbon nanotubes were covalently functionalized with l-histidine (His–MWNTs) as online pseudospecific affinity adsorbent for immunoglobulin G (IgG) separation and purification with a simple surface modification method, using 1-ethyl-3-(3-dimethyaminopropyl) carbodiimide hydrochloride (EDC) and N-hydroxysuccinimde (NHS). The affinity of the His–MWNTs toward IgG was investigated...
An electrochemical sensor for the determination of the chlorophenoxy herbicide MCPA has been developed, based on a combination of multi-walled carbon nanotubes with incorporated β-cyclodextrin and a polyaniline film modified glassy carbon electrode. The proposed molecular host–guest recognition based sensor has a high electrochemical sensitivity for the determination of MCPA. The electrochemical behaviour...
A 3α-hydrosteroid biosensor for androsterone determination has been prepared by immobilizing the enzyme 3α-hydroxysteroid dehydrogenase (3α-HSD) in a composite electrode platform constituted of a mixture of multi-walled carbon nanotubes (MWCNTs), octylpyridinium hexafluorophosphate (OPPF 6 ) ionic liquid and NAD + cofactor. This configuration allowed the fast, sensitive and stable...
In this paper, an effective and simple method was used for the immobilization of single wall carbon nanotubes (SWCNTs) on a monolithic HPLC material containing 2μm macropore sizes and 13nm mesopore sizes. The chromatographic support was coated with ultra short SWCNTs in a noncovalent way to preserve the sp 2 nanotube structure and thus their physico–chemical properties. It was demonstrated...
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