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Sections of a 13Cr supermartensitic stainless steel were investigated to determine the optimum sample preparation for measurement of the austenite content by X-ray diffraction. The surface of several samples was mechanically ground or polished using media of grit sizes in the range 1–120μm. The strained surface layer was afterwards removed stepwise by electropolishing, and the austenite content measured...
This paper aims to explore the impact of the parameters such as pH of the system, refluxing temperature, water quantity and chemical composition on the sol–gel synthesis of lithium-mica glass-ceramic nano-powder. The synthesis process was accomplished using two chemical composition formula (Li(1+x)Mg3AlSi3(1+x)O10+6.5xF2 and LiMg3AlSi3(1+x)O10+6xF2). X-ray diffraction, Brunauer–Emmett–Teller surface...
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