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An improved method for the sol–gel synthesis of binary (TiO 2 ) 0.5 (P 2 O 5 ) 0.5 glasses has been developed. Elemental analysis of the products showed that the loss of phosphorous upon drying and heat treatment is low. The structure of the heat-treated glasses was studied using neutron diffraction and high-energy X-ray diffraction, analysis of which revealed...
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