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Sodium intercalation compounds of HfNCl have been prepared at room temperature in naphtyl sodium solutions in tetrahydrofuran and their crystal structure has been investigated by Rietveld refinement using X-ray powder diffraction data and high-resolution electron microscopy. The structure of two intercalates with space group R3¯m and lattice parameters a=3.58131(6)Å, c=57.752(6)Å, and a=3.58791(8)Å,...
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