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Intermetallic NiAl bonded sub-stoichiometric titanium carbide based composite of TiC 0.6 /NiAl was fabricated by a two-step melt infiltration processing method, and its microstructure was characterized with scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HRTEM). Ordered Ni 2 AlTi precipitated in NiAl matrix and a new long period modulated structure as a transition layer appeared at the phase boundary.