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Capillary gas chromatography (CGC) in combination with mass spectrometry (MS) was optimized for the separation and detection of the fatty acids occurring in the lipid fraction of blood. A fingertip blood sample (ca. 50μL) was transesterified into the methyl esters and analyzed on a 100m×0.25mm ID column coated with a biscyanopropyl polysiloxane (HP-88) stationary phase. The method was retention time...
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