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The photocatalytic oxidative degradation of 2-methylthiophene has been investigated in aqueous suspensions of TiO 2 . The nature of the degradation products was investigated using GC/MS. The effects of the nature of the solvent and type of radiation have also been examined. In the degradation of 2-methylthiophene several intermediates were detected including hydroxythiophenes, various dimeric and trimeric structures.