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New cation-deficient solid solutions of Ca3–1.5xYbx□0.5xB2SiO8 (x = 0–0.4) based on Ca3B2SiO8 borosilicate were synthesized. It was found that solid solutions in the range 0 ≤ x < 0.125 are structurally similar to the low-temperature monoclinic β-Ca3B2SiO8, whereas those of the range 0.187 < x < 0.4 are similar to the high-temperature orthorhombic α-Ca3B2SiO8. The crystal structures of solid...
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