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The Fe x (Cr 2 O 3 ) 1−x system, with 0.10≤X≤0.80, was mechanically processed for 24h in a high-energy ball-mill. In order to examine the possible formation of iron–chromium oxides and alloys, the milled samples were, later, thermally annealed in inert (argon) and reducing (hydrogen) atmospheres. The as-milled and annealed products were characterized by X-ray diffraction,...
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