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Extremely high diastereomeric excess was achieved from the photosensitized polar addition of methanol to (R)-(+)-limonene 1. Diastereomeric excess was varied from 28.1 to 96.3% depending on the solvent polarity, reaction temperature, and structure of sensitizer.
Department of Chemistry, Center for Molecular Design and Synthesis and School of Molecular Science-BK21, Korea Advanced Institute of Science and Technology, Yusung-Gu, Taejon 305-701, South Korea
Department of Chemistry, Center for Molecular Design and Synthesis and School of Molecular Science-BK21, Korea Advanced Institute of Science and Technology, Yusung-Gu, Taejon 305-701, South Korea