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Monolithic Al2O3-SiO2-TiO2 with multiscale porous structures has been prepared via a sol-gel process accompanied by phase separation. Poly(ethylene oxide) (PEO) is used to induce the phase separation and formamide (FA) to control the gelation of ternary system. The dried gel is amorphous. After heat treatment at 1050°C, the gel transforms into the phase Al4Ti2SiO12. The interconnected macropores are...
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